Issue

Vol. 17 (2025)

Tailoring Artificial Solid Electrolyte Interphase via MoS2 Sacrificial Thin Film for Li-Free All-Solid-State Batteries

https://doi.org/10.1007/s40820-025-01729-w
Dong‑Bum Seo
Thin Film Materials Research Center, Korea Research Institute of Chemical Technology (KRICT), 141 Gajeong‑ro, Yuseong‑gu, Daejeon 34114, Republic of Korea
Dohun Kim
Department of Materials Science and Engineering, Chungnam National University, Daejeon 34134, Republic of Korea
Mee‑Ree Kim
Department of Materials Science and Engineering, Chungnam National University, Daejeon 34134, Republic of Korea
Jimin Kwon
Department of Materials Science and Engineering, Chungnam National University, Daejeon 34134, Republic of Korea
Hyeong Jun Kook
Intelligent Sensors Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Saewon Kang
Thin Film Materials Research Center, Korea Research Institute of Chemical Technology (KRICT), 141 Gajeong‑ro, Yuseong‑gu, Daejeon 34114, Republic of Korea
Soonmin Yim
Thin Film Materials Research Center, Korea Research Institute of Chemical Technology (KRICT), 141 Gajeong‑ro, Yuseong‑gu, Daejeon 34114, Republic of Korea
Sun Sook Lee
Thin Film Materials Research Center, Korea Research Institute of Chemical Technology (KRICT), 141 Gajeong‑ro, Yuseong‑gu, Daejeon 34114, Republic of Korea
Dong Ok Shin
Intelligent Sensors Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Ki‑Seok An
Thin Film Materials Research Center, Korea Research Institute of Chemical Technology (KRICT), 141 Gajeong‑ro, Yuseong‑gu, Daejeon 34114, Republic of Korea
Sangbaek Park
Department of Materials Science and Engineering, Chungnam National University, Daejeon 34134, Republic of Korea

Corresponding Author: Sangbaek Park

sb.park@cnu.ac.kr

Nano-Micro Letters, Vol. 17 (2025), Article Number: 224

Abstract

Anode-free all-solid-state batteries (AFASSBs) are potential candidates for next-generation electric mobility devices that offer superior energy density and stability by eliminating Li from the anode. However, despite its potential to stabilize the interface between sulfide solid electrolytes (SEs) and anode-free current collectors (CCs) efficiently, a controllable approach to incorporating MoS2 into AFASSBs has not yet been found. Herein, we propose a strategy for stabilizing the interface of Li-free all-solid-state batteries using controllable MoS2 sacrificial thin films. MoS2 was controllably grown on CCs by metal–organic chemical vapor deposition, and the MoS2 sacrificial layer in contact with the SEs formed an interlayer composed of Mo metal and Li2S through a conversion reaction. In the AFASSBs with MoS2, Mo significantly reduces the nucleation overpotential of Li, which results in uniform Li plating. In addition, MoS2-based Li2S facilitates the formation of a uniform and robust SE interface, thereby enhancing the stability of AFASSBs. Based on these advantages, cells fabricated with MoS2 exhibited better performance as both asymmetrical and full cells with LiNi0.6Co0.2Mn0.2O2 cathodes than did cells without MoS2. Moreover, the cell performance was affected by the MoS2 size, and full cells having an optimal MoS2 thickness demonstrated a 1.18-fold increase in the initial discharge capacity and a sevenfold improvement in capacity retention relative to SUS CCs. This study offers a promising path for exploiting the full potential of MoS2 for interface stabilization and efficient AFASSB applications.


Highlights:
1 We present the first-ever fabrication of the anode-free all-solid-state battery (AFASSB) structure using a MoS2 sacrificial layer.
2 The addition of an MoS2 sacrificial layer to AFASSBs could decrease the nucleation overpotential of Li and enable favorable Li formation at the interface owing to the formation of an interlayer comprising Li2S and Mo metal.
3 The AFASSB full cell assembled with LiNi0.6Co0.2Mn0.2O2 cathodes operated successfully, demonstrating superior cycling stability and enhanced capacity relative to the cells with SUS.

Keywords

Molybdenum disulfide Anode-free all-solid-state battery Li-free all-solid-state battery Mo metal Lithium sulfide
Seo, Dong‑Bum, Dohun Kim, Mee‑Ree Kim, Jimin Kwon, Hyeong Jun Kook, Saewon Kang, Soonmin Yim, Sun Sook Lee, Dong Ok Shin, Ki‑Seok An, and Sangbaek Park. 2025. “Tailoring Artificial Solid Electrolyte Interphase via MoS2 Sacrificial Thin Film for Li-Free All-Solid-State Batteries”. Nano-Micro Letters 17 (April):224. https://doi.org/10.1007/s40820-025-01729-w.
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