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Vol. 18 (2026)

Growth-Directing Nanostructured Interfaces via Block Copolymer-Templated Au Nanoseed Arrays for Stabilized Zinc Anodes in Lean-Zinc Batteries

https://doi.org/10.1007/s40820-026-02167-y
Dong Won Hae
Smart Materials Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Hoseok Lee
Department of Future Energy Engineering, Sungkyunkwan University, Suwon 16419, Republic of Korea
Hyeong Jun Kook
Smart Materials Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Ga Hee Kim
Smart Materials Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Saehun Kim
Smart Materials Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Jaecheol Choi
Smart Materials Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Min Pyeong Kim
Smart Materials Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Seok Hun Kang
Smart Materials Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Won Jun Lee
Department of Fiber System Engineering, Dankook University, Yongin 16890, Republic of Korea
Young‑Gi Lee
Smart Materials Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea
Hyeong Min Jin
Department of Organic Materials Engineering, Chungnam National University, Daejeon 34134, Republic of Korea
Jongsoon Kim
Department of Future Energy Engineering, Sungkyunkwan University, Suwon 16419, Republic of Korea
Dong Ok Shin
Smart Materials Research Section, Electronics and Telecommunications Research Institute (ETRI), Daejeon 34129, Republic of Korea

Corresponding Author: Dong Ok Shin

doshin@etri.re.kr

Nano-Micro Letters, Vol. 18 (2026), Article Number: 355

Abstract

Achieving dendrite-free and highly reversible Zn anodes remains a critical challenge for realizing high-performance aqueous Zn-ion batteries (AZIBs). Here, we report a rationally designed nanoscale interfacial architecture, constructed via sequential assembly of a reduced graphene oxide (rGO) nanolayer and solvent-annealed block copolymer (BCP)-templated Au nanoseed arrays, that enables spatially uniform Zn nucleation and planar plating, yielding highly stable, dendrite-free Zn anodes with minimal excess Zn. The synergistic integration of zincophilic Au nanoseeds on rGO, which energetically favor Zn (002) nucleation, effectively suppresses parasitic reactions and directs preferentially oriented Zn growth, yielding macroscopically uniform Zn plating with an exceptionally high (002) relative texture coefficient (RTC) of 88.2%. Combined experimental and theoretical investigations reveal that the homogeneous Zn2+ flux and substrate-induced texture development at the Au nanoseed–rGO interface (AGI) are critical for directing initial Zn nucleation and sustaining planar growth. The plated Zn on AGI (Zn@AGI) delivers exceptional cycling stability (> 3000 h at 1 mA cm−2, 10% DOD) and excellent performance under high-DOD conditions. Moreover, full cells incorporating Zn@AGI achieve a remarkably high energy density of 156.1 Wh kg−1 full electrode under an ultralow N/P ratio of 2. This work presents a strategic interfacial approach toward stable and practical AZIBs.


Highlights:
1 A nanoscale Au nanoseed–rGO interface (AGI) architecture drives highly planar Zn plating with an exceptional (002) texture (RTC = 88.2%), yielding dense and dendrite-free Zn growth.
2 The AGI-driven texture regulation homogenizes Zn2+ flux, suppresses ZHS/HER side reactions and delivers exceptional cycling durability (>3000 h at 10% depth of discharge).
3 A full-cell paired with a high-loading MnO2 cathode delivers 156.1 Wh kg−1 under an ultralow N/P ratio of 2, highlighting strong practical viability for lean-zinc batteries.

Keywords

Aqueous zinc-ion battery Block copolymer template Au nanoseed Plated zinc anode
Hae, Dong Won, Hoseok Lee, Hyeong Jun Kook, Ga Hee Kim, Saehun Kim, Jaecheol Choi, Min Pyeong Kim, Seok Hun Kang, Won Jun Lee, Young‑Gi Lee, Hyeong Min Jin, Jongsoon Kim, and Dong Ok Shin. 2026. “Growth-Directing Nanostructured Interfaces via Block Copolymer-Templated Au Nanoseed Arrays for Stabilized Zinc Anodes in Lean-Zinc Batteries”. Nano-Micro Letters 18 (May):355. https://doi.org/10.1007/s40820-026-02167-y.
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