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Vol. 17 (2025)

Boosting Alcohol Oxidation Electrocatalysis with Multifactorial Engineered Pd1/Pt Single-Atom Alloy-BiOx Adatoms Surface

https://doi.org/10.1007/s40820-025-01678-4
Yujia Liao
Shenzhen Key Laboratory of Energy Electrocatalytic Materials, Guangdong Provincial Key Laboratory of New Energy Materials Service Safety, College of Materials Science and Engineering, Shenzhen University, Shenzhen 518055, People’s Republic of China
Wen Chen
Shenzhen Key Laboratory of Energy Electrocatalytic Materials, Guangdong Provincial Key Laboratory of New Energy Materials Service Safety, College of Materials Science and Engineering, Shenzhen University, Shenzhen 518055, People’s Republic of China
Yutian Ding
Shenzhen Key Laboratory of Energy Electrocatalytic Materials, Guangdong Provincial Key Laboratory of New Energy Materials Service Safety, College of Materials Science and Engineering, Shenzhen University, Shenzhen 518055, People’s Republic of China
Lei Xie
Shenzhen Key Laboratory of Energy Electrocatalytic Materials, Guangdong Provincial Key Laboratory of New Energy Materials Service Safety, College of Materials Science and Engineering, Shenzhen University, Shenzhen 518055, People’s Republic of China
Qi Yang
Department of Chemistry, City University of Hong Kong, Kowloon 999077, People’s Republic of China
Qilong Wu
Department of Chemistry, Southern University of Science and Technology (SUSTech), Shenzhen 518055, People’s Republic of China
Xianglong Liu
Shenzhen Key Laboratory of Energy Electrocatalytic Materials, Guangdong Provincial Key Laboratory of New Energy Materials Service Safety, College of Materials Science and Engineering, Shenzhen University, Shenzhen 518055, People’s Republic of China
Jinliang Zhu
School of Resources, Environment and Materials, MOE Key Laboratory of New Processing Technology for Nonferrous Metals and Materials, Guangxi University, Nanning 530004, People’s Republic of China
Renfei Feng
Canadian Light Source Inc., 44 Innovation Blvd., Saskatoon, SK S7N 0×4, Canada
Xian‑Zhu Fu
Shenzhen Key Laboratory of Energy Electrocatalytic Materials, Guangdong Provincial Key Laboratory of New Energy Materials Service Safety, College of Materials Science and Engineering, Shenzhen University, Shenzhen 518055, People’s Republic of China
Shuiping Luo
Shenzhen Key Laboratory of Energy Electrocatalytic Materials, Guangdong Provincial Key Laboratory of New Energy Materials Service Safety, College of Materials Science and Engineering, Shenzhen University, Shenzhen 518055, People’s Republic of China
Jing‑Li Luo
Shenzhen Key Laboratory of Energy Electrocatalytic Materials, Guangdong Provincial Key Laboratory of New Energy Materials Service Safety, College of Materials Science and Engineering, Shenzhen University, Shenzhen 518055, People’s Republic of China

Corresponding Author: Shuiping Luo

luosp@szu.edu.cn

Nano-Micro Letters, Vol. 17 (2025), Article Number: 172

Abstract

Engineering nanomaterials at single-atomic sites could enable unprecedented catalytic properties for broad applications, yet it remains challenging to do so on the surface of multimetallic nanocrystals. Herein, we present the multifactorial engineering (size, shape, phase, and composition) of the fully ordered PtBi nanoplates at atomic level, achieving a unique catalyst surface where the face-centered cubic (fcc) Pt edges are modified by the isolated Pd atoms and BiOx adatoms. This Pd1/Pt-BiOx electrocatalyst exhibits an ultrahigh mass activity of 16.01 A mg−1Pt+Pd toward ethanol oxidation in alkaline electrolyte and enables a direct ethanol fuel cell of peak power density of 56.7 mW cm−2. The surrounding BiOx adatoms are critical for mitigating CO-poisoning on the Pt surface, and the Pd1/Pt single-atom alloy further facilitates the electrooxidation of CH3CH2OH. This work offers new insights into the rational design and construction of sophisticated catalyst surface at single-atomic sites for highly efficient electrocatalysis.


Highlights:
1 A unique catalyst surface where ultrathin Pt edges are modified by the isolated Pd atoms and BiOx adatoms is rational designed and achieved.
2 The Pd1/Pt-BiOx electrocatalyst exhibits an ultrahigh mass activity of 16.01 A mg−1Pt+Pd toward ethanol oxidation and enables a direct ethanol fuel cell of peak power density of 56.7 mW cm−2.
3 The surrounding BiOx adatoms are critical for mitigating CO-poisoning on Pt surface, and the Pd1/Pt single-atom alloy further facilitates the electrooxidation of CH3CH2OH.

Keywords

Electrocatalysis Alcohol oxidation Single-atom alloy Intermetallic Fuel cell
Liao, Yujia, Wen Chen, Yutian Ding, Lei Xie, Qi Yang, Qilong Wu, Xianglong Liu, Jinliang Zhu, Renfei Feng, Xian‑Zhu Fu, Shuiping Luo, and Jing‑Li Luo. 2025. “Boosting Alcohol Oxidation Electrocatalysis With Multifactorial Engineered Pd1/Pt Single-Atom Alloy-BiOx Adatoms Surface”. Nano-Micro Letters 17 (March):172. https://doi.org/10.1007/s40820-025-01678-4.
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