Issue

Vol. 1 No. 1 (2009)

Synthesis of Ni nanowires via a hydrazine reduction route in aqueous ethanol solutions assisted by external magnetic fields

https://doi.org/10.1007/BF03353607
Liying Zhang
National Key Laboratory of Nano/Micro Fabrication Technology, Key Laboratory for Thin Film and Microfabrication of Ministry of Education, Institute of Micro and Nano Science and Technology, Shanghai Jiao Tong University, Shanghai 200240, China
Jian Wang
National Key Laboratory of Nano/Micro Fabrication Technology, Key Laboratory for Thin Film and Microfabrication of Ministry of Education, Institute of Micro and Nano Science and Technology, Shanghai Jiao Tong University, Shanghai 200240, China
Liangming Wei
National Key Laboratory of Nano/Micro Fabrication Technology, Key Laboratory for Thin Film and Microfabrication of Ministry of Education, Institute of Micro and Nano Science and Technology, Shanghai Jiao Tong University, Shanghai 200240, China
Ping Liu
National Key Laboratory of Nano/Micro Fabrication Technology, Key Laboratory for Thin Film and Microfabrication of Ministry of Education, Institute of Micro and Nano Science and Technology, Shanghai Jiao Tong University, Shanghai 200240, China
Hao Wei
National Key Laboratory of Nano/Micro Fabrication Technology, Key Laboratory for Thin Film and Microfabrication of Ministry of Education, Institute of Micro and Nano Science and Technology, Shanghai Jiao Tong University, Shanghai 200240, China
Yafei Zhang
National Key Laboratory of Nano/Micro Fabrication Technology, Key Laboratory for Thin Film and Microfabrication of Ministry of Education, Institute of Micro and Nano Science and Technology, Shanghai Jiao Tong University, Shanghai 200240, China

Corresponding Author: Yafei Zhang

yfzhang@sjtu.edu.cn

Nano-Micro Letters, Vol. 1 No. 1 (2009), Article Number: 49-52

Abstract

One-dimensional Ni nanostructures were synthesized via a hydrazine reduction route under external magnetic fields. The mixture of de-ionized water and ethanol was used as the reaction solvent and hydrazine hydrate as reducing agents. The morphology and properties of Ni nanostructures were characterized by X-ray diffractometer (XRD), scanning electron microscopy (SEM), and vibrating sample magnetometer (VSM). It was found that the magnetic field strength, concentration of Ni ions, reaction time and temperature as well as pH values played key roles on formation, microstructures and magnetic properties of Ni nanowires. The optimal wires have diameter of ∼200 nm and length up to ∼200 μm. And their coercivity is ∼260 Oe, which is much larger than the commercial Ni powders of 31 Oe. This work presents a simple, low-cost, environment-friendly and large-scale production approach to fabricate one-dimensional magnetic materials. The resulting materials may have potential applications in conductive filters, magnetic sensors and catalytic agents.

Keywords

Ni fiber Hydrazine reduction Magnetic field Magnetic properties
Zhang, Liying, Jian Wang, Liangming Wei, Ping Liu, Hao Wei, and Yafei Zhang. 2009. “Synthesis of Ni Nanowires via a Hydrazine Reduction Route in Aqueous Ethanol Solutions Assisted by External Magnetic Fields”. Nano-Micro Letters 1 (1):49-52. https://doi.org/10.1007/BF03353607.
Download Citation
Endnote/Zotero/Mendeley (RIS)
BibTeX
References
  1. W. Zhou and L. Guo, Chem. Bull. 69, w063 (2006).
  2. L. Tan, Q. Li, Y. Yang, F. Li, L. Liu and M. Li, Mater. Rev. 17, 41 (2003).
  3. L. Tan, Q. Li, Y. Yang, F. Li, L. Liu and M. Li, J. Solid Rocket Technol. 27, 198 (2004).
  4. M. A. Ermakova, D. Y. Ermakov, S. V. Cherepanova and L. M. Plyasova, J. Phys. Chem. B 106, 11922 (2002). doi:10.1021/jp021231q
  5. J. Bao, C. Tie, Z, Xu, Q. Zhou, D. Shen and Q. Ma, Adv. Mater. 13, 1631 (2001).
  6. S. Z. Chu, K. Wada, S. Inoue and S. Todoroki, Chem. Mater. 14, 4595 (2002). doi:10.1021/cm020272w
  7. E. K. Athanassiou, P. Grossmann, R. N. Grass and W. Stark, J. Nanotech. 18, 165606 (2007).
  8. M. Tanase, L. A. Bauer, A. Hultgren, D. M. Silevitch, L. Sun, D. H. Reich, P. C. Searson and G. J. Meyer, Nano Lett. 1, 155 (2001). doi:10.1021/nl005532s
  9. H. Pan, B. Liu, J. Yi, C. Poh, S. Lim, J. Ding, Y. Feng, C. H. A. Huan and J. Lin, J. Phys. Chem. B 109, 3094 (2005). doi:10.1021/jp0451997
  10. S. Z. Chu, K. Wada, S. Inoue, S. Todoroki, Y. K. Takahashi and K. Hono, Chem. Mater. 14, 4595 (2002). doi:10.1021/cm020272w.
  11. M. Knez, A. M. Bittner, F. Boes, C. Wege, H. Jeske, E. Maib and K. Kern, Nano Lett. 3, 1079 (2003). doi:10.1021/nl0342545
  12. H. Niu, Q. Chen, M. Ning, Y. Jia and X. Wang, J. Phys. Chem. B 108, 3996 (2004). doi:10.1021/jp0361172
  13. J. Qin, J. Nogues, M. Mikhaylova, A. Roig, J. S. Munoz and M. Muhammed, Chem. Mater. 17, 1829 (2005). doi:10.1021/cm047870q
  14. H. Q. Cao, L. D. Wang, Y. Qiu, Q. Z. Wu, G. Z. Wang, L. Zhang and X. W. Liu, Chem. Phys. Chem. 7, 1500 (2006). doi:10.1002/cphc.200500690
  15. S. H. Ge, C. Li, X. Ma, W. Li, L. Xi and C. X. Li, J. Appl. Phys. 90, 509 (2001). doi:10.1063/1.1327599
  16. I. W. Hamley, Nanotechnology 14, R39 (2003).
  17. H. M. Luo, D. H. Wang, J. B. He and Y. F. Lu, J. Phys. Chem. B 109, 1919 (2005). doi:10.1021/jp045554t
  18. F. L. Jia, L. Z. Zhang, X. Y. Shang and Y. Yang. Adv. Mater. 20, 1050 (2008). doi:10.1002/adma.200702159
Read More
Author biographies are not available.
Download this PDF file
PDF
Statistic
Read Counter : 2517 Download : 1914

Most read articles by the same author(s)

<< < 1 2 3